Allyl Mercaptan → HCID 21217670, Verbindung

HRID 1586001Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1586001
[Na].[CH2:2]([SH:5])[CH:3]=[CH2:4].[CH2:6]([O:11][C:12]1[N:13]=[N:14][C:15](Cl)=[CH:16][CH:17]=1)[CH2:7][CH:8]([CH3:10])[CH3:9]>CO>[CH2:6]([O:11][C:12]1[N:13]=[N:14][C:15]([S:5][CH2:2][CH:3]=[CH2:4])=[CH:16][CH:17]=1)[CH2:7][CH:8]([CH3:10])[CH3:9]

Komponenten

5

Edukt 3

HCID 13367Allyl MercaptanHCID 2528263-Chloro-6-(3-methylbutoxy)pyridazineHCID 5360545Sodium

Produkt 1

HCID 21217670HCID 21217670, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

1.15 g(0.05 mol) of metallic sodium was dissolved in 150 ml of absolute methanol and then mixed with 4.98 ml(0.05 mol) of allylmercaptan. To this mixture was added 10.03 g(0.05 mol) of 3-isopentyloxy-6-chloropyridazine. The reaction solution was refluxed for 24 hours and then treated according to the same manner as Example 1 to obtain the title compound as a pale yellow oil.

Aufarbeitung

  1. temperatureThe reaction solution was refluxed for 24 hours
  2. additiontreated

Quellen und Nachweise

ORD-Eintrag
ord-05db89f258dd44e4a3c0f0f4bce562e8
Quelldatensatz
uspto-grants-1999_08
Patentnummer
US05942511

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