Allyl Mercaptan → HCID 10219981, Verbindung

HRID 1586002Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1586002
[Na].[CH2:2]([SH:5])[CH:3]=[CH2:4].[OH:6][CH2:7][CH2:8][O:9][C:10]1[N:11]=[N:12][C:13](Cl)=[CH:14][CH:15]=1>CO>[OH:6][CH2:7][CH2:8][O:9][C:10]1[N:11]=[N:12][C:13]([S:5][CH2:2][CH:3]=[CH2:4])=[CH:14][CH:15]=1

Komponenten

5

Edukt 3

HCID 13367Allyl MercaptanHCID 5360545SodiumHCID 14343567122913-80-8

Produkt 1

HCID 10219981HCID 10219981, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

0.23 g(0.01 mol) of metallic sodium was dissolved in 30 ml of absolute methanol and then mixed with 1.00 ml(0.01 mol) of allylmercaptan. To this mixture was added 1.75 g(0.01 mol) of 3-(2-hydroxyethoxy)-6-chloropyridazine. The reaction solution was refluxed for 24 hours and then treated according to the same manner as Example 1 to obtain the title compound as a pale white needle crystal.

Aufarbeitung

  1. temperatureThe reaction solution was refluxed for 24 hours
  2. additiontreated

Quellen und Nachweise

ORD-Eintrag
ord-fd34e192f5ca401d8e966cabc950c911
Quelldatensatz
uspto-grants-1999_08
Patentnummer
US05942511

Notizen zur Reaktion

Wird geladen…