HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1586684Erstellt: 27. Oktober 2026
Imidazole → 1-[[3-[[3-(Hexadecyloxy)-2-methoxypropoxy]methyl]phenyl]methyl]-1H-imidazol
https://huagongshe.com/reaction/1586684
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Imidazole | HCID 795 | — |
| Edukt | 1-(Bromomethyl)-3-[[3-(hexadecyloxy)-2-methoxypropoxy]methyl]benzene | HCID 19939557 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | 1-[[3-[[3-(Hexadecyloxy)-2-methoxypropoxy]methyl]phenyl]methyl]-1H-imidazol | HCID 19939546 | 86,3% |
Reaktionsschritte
A mixture of 2.4 g of 1-(bromomethyl)-3-[[3-(hexadecyloxy)-2-methoxypropoxy]methyl]benzene, 2.54 g of imidazole and 30 ml of toluene was heated at 80° C. under argon in a pressure bottle for 4 hours and then evaporated. The residue was purified by chromatography, giving 2.02 g of the desired product as a colorless oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US05215975 |
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| Quelldatensatz | uspto-grants-1993_06 |
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| ORD ID | ord-d149b267b51b42b785b078fb59b9c62d |
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| Quellennotiz | uspto-grants-1993_06 |
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