Pyridine → HCID 6475484, Verbindung
Reaktionsgleichung
[CH3:1][C:2]1[C:8](=[O:9])[NH:7][C:5](=[O:6])[N:4]([C@@H:10]2[O:14][C@H:13]([CH2:15][OH:16])[C@@H:12]([N:17]=[N+:18]=[N-:19])[CH2:11]2)[CH:3]=1.N1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1>>[CH3:21][CH2:22][CH2:23][CH2:24][CH2:25]/[CH:25]=[CH:24]\[CH2:23]/[CH:22]=[CH:21]\[CH2:25][CH2:24][CH2:23][CH2:22][CH2:21][CH2:1][CH2:2][C:8]([O:16][CH2:15][C@H:13]1[O:14][C@@H:10]([N:4]2[C:5](=[O:6])[NH:7][C:8](=[O:9])[C:2]([CH3:1])=[CH:3]2)[CH2:11][C@@H:12]1[N:17]=[N+:18]=[N-:19])=[O:9]Komponenten
3
Versuchsvorschrift
The procedure for this preparation is exactly as above. The quantities used were as follows: AZT, 0.723 g, 2.70 mmol. LA acid chloride, 1.3 g, 4.36 mmol. 10 ml of anhydrous pyridine. Yield, 54% (0.770 g, 1.458 mmol).
Aufarbeitung
- customYield
Quellen und Nachweise
- ORD-Eintrag
- ord-7b3978d9d4b54e19b3e20d31902fc0ea
- Quelldatensatz
- uspto-grants-1993_06