1,3-Dimethyl-2-imidazolidinone → 1-(2-Cyanophenyliminomethyl)-2-nitroiminoimidazolidine

Beteiligte Stoffe

Reaktionsschritte

0.05 g of SnCl4 was added to a mixture of 2.0 g of 1-diethoxymethyl-2-nitroiminoimidazolidine, 1.02 g of o-aminobenzonitrile and 5 ml of 1,3-dimethyl-2-imidazolidinone, followed by agitation at room temperature for 10 minutes. Ether was added to the reaction mixture, and the resultant crystals were collected by filtration and dried to give 2.9 g of 1-(2-cyanophenyliminomethyl)-2-nitroimino-imidazolidine.

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