HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Pyrrolidone → 1-[3-(2-Hydroxyethyl)phenyl]-2-pyrrolidinone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Pyrrolidone | HCID 12025 | — |
| Edukt | 2-(3-Bromophenyl)ethan-1-ol | HCID 2734090 | — |
| Produkt | 1-[3-(2-Hydroxyethyl)phenyl]-2-pyrrolidinone | HCID 57444361 | 15% |
Reaktionsschritte
The title compound was prepared in 15% yield according to the general procedure for the preparation of the amides, ureas and carbamates (Method A) starting from 2-(3-bromophenyl)ethanol and 2-pyrrolidinone. Purification was achieved by flash chromatography on silica gel eluting with ethyl acetate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07732600B2 |
| Quelldatensatz | uspto-grants-2010_06 |
| ORD ID | ord-bbab621c1e3b4c94b45ab537ff5a5d8b |
| Quellennotiz | uspto-grants-2010_06 |