HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Triethylamine → Cobalt octoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Triethylamine | HCID 8471 | — |
| Edukt | Cobalt dinitrate | HCID 25000 | — |
| Edukt | 3-Ethylheptanoic acid | HCID 139715 | — |
| Lösungsmittel | Cyclohexane | HCID 8078 | — |
| Produkt | Cobalt octoate | HCID 8696 | 55,5% |
Reaktionsschritte
Using a 1 liter flask, 0.40 mol triethylamine is added with stirring at room temperature to 0.40 mol 2-ethyl hexane carboxylic acid. After the exothermic reaction has abated, the reaction mixture is diluted with 65 ml cyclohexane and 0.20 mol cobalt nitrate is added. After stirring for 30 minutes, the reaction solution is filtered, leaving a 55.5% blue cobalt octoate solution in cyclohexane.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05220045 |
| Quelldatensatz | uspto-grants-1993_06 |
| ORD ID | ord-ae8fdf9f837b4f1f9f9691ad0a891fb6 |
| Quellennotiz | uspto-grants-1993_06 |