HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-(Pyridin-2-yl)ethan-1-amine → tert-Butyl 4-((1-(pyridin-2-yl)ethyl)amino)piperidine-1-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-(Pyridin-2-yl)ethan-1-amine | HCID 541877 | — |
| Edukt | tert-Butyl 4-oxopiperidine-1-carboxylate | HCID 735900 | — |
| Edukt | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | tert-Butyl 4-((1-(pyridin-2-yl)ethyl)amino)piperidine-1-carboxylate | HCID 60137113 | — |
Reaktionsschritte
Using General Procedure B: Reaction of 1-Pyridin-2-yl-ethylamine and 1-Boc-4-piperidone with NaBH(OAc)3 in CH2Cl2 gave 4-(1-Pyridin-2-yl-ethylamino)-piperidine-1-carboxylic acid tert-butyl ester as a colorless oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07291631B2 |
| Quelldatensatz | uspto-grants-2007_11 |
| ORD ID | ord-5433f5bba68a4fe7a43e85e37e3a78c2 |
| Quellennotiz | uspto-grants-2007_11 |