Hexafluoropropene oxide trimer → CF3(CF2)2Ocf(CF3)CF2ocf(CF3)cooch2CH(CH3)O(CH2)3ococf(CF3)-ocf2CF(CF3)O(CF2)2CF3

HRID 1594456Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1594456
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Komponenten

4

Edukt 2

HCID 102863Hexafluoropropene oxide trimerHCID 217585032-(3-Hydroxypropoxy)propan-1-ol

Produkt 1

HCID 131726696CF3(CF2)2Ocf(CF3)CF2ocf(CF3)cooch2CH(CH3)O(CH2)3ococf(CF3)-ocf2CF(CF3)O(CF2)2CF3

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 516892Sodium BicarbonateLösungsmittel

Versuchsvorschrift

CF3(CF2)2OCF(CF3)CF2OCF(CF3)COF (120.69 g) was loaded into an autoclave and stirred under a nitrogen stream, and HO(CH2)3OCH(CH3)CH2OH (15.1 g) prepared in Example 2-3 was fed over 2 hours, while the temperature in the autoclave was maintained at 30° C. or below. Then, the reaction solution was stirred at room temperature under a nitrogen stream overnight and poured onto saturated aqueous NaHCO3 (500 mL) with ice.

Aufarbeitung

  1. temperaturewas maintained at 30° C. or below
  2. waitstream overnight

Quellen und Nachweise

ORD-Eintrag
ord-6d28ae8fa6544650b20af4703147145a
Quelldatensatz
uspto-grants-2007_11
Patentnummer
US07301052B2

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