Hydrochloric Acid → Phenyl octanoate

HRID 1599522Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1599522
[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:8](O)(=[O:16])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15].S(=O)=O.Cl>S(Cl)(Cl)=O>[C:8]([O:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)(=[O:16])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15]

Komponenten

6

Edukt 4

HCID 313Hydrochloric AcidHCID 379Octanoic AcidHCID 996PhenolHCID 1119Sulfur Dioxide

Produkt 1

HCID 229895Phenyl octanoate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 24386Thionyl ChlorideLösungsmittel

Versuchsvorschrift

The ester was prepared by slowly adding thionyl chloride (10 ml) to a mixture of pure phenol (6.5 g) and octanoic acid (10 g). The reaction mixture was warmed to drive off the sulfur dioxide and hydrogen chloride gases. The crude mixture was distilled at 95°-100° C./5 mmHg.

Aufarbeitung

  1. temperatureThe reaction mixture was warmed
  2. distillationThe crude mixture was distilled at 95°-100° C./5 mmHg

Quellen und Nachweise

ORD-Eintrag
ord-2c67f39815a040c1b539b782c2b2c497
Quelldatensatz
uspto-grants-1998_04
Patentnummer
US05741821

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