HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Triethanolamine → Triethanolamine hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Triethanolamine | HCID 7618 | — |
| Edukt | Carbonochloridate | HCID 21226386 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | Triethanolamine hydrochloride | HCID 101814 | — |
Reaktionsschritte
100 g of a polyether acrylate (Laromer® LR 8812) were admixed with 5.75 g of chloroformate of the formula III and 3.3 g of triethanolamine at room temperature. 300 ml of ethyl acetate were then added. After 2 hours, the triethanolammonium chloride formed was washed out using distilled water in a separating funnel. After removal of the aqueous phase, the ethyl acetate was distilled off. (Viscosity of the end product: 928 mPas).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05741829 |
| Quelldatensatz | uspto-grants-1998_04 |
| ORD ID | ord-33c9d01a63354c51baec4eb8772bdcac |
| Quellennotiz | uspto-grants-1998_04 |