Chlorotrimethylsilane → N,N-Diethyl-2-(trimethylsilyl)-1-naphthalenecarboxamide

Beteiligte Stoffe

Reaktionsschritte

N,N-Diethyl-1-naphthalenecarboxamide was reacted with 2 eq TMSCl according to General Method A. The resulting reaction mixture was worked up in the usual manner, then purified by chromatography with 20% ethyl acetate/80% hexanes to afford 2.1 g of the desired compound as a clear oil, a 71% yield.

Herkunft & Nachweise