Chlorotrimethylsilane → N-Ethyl-2-(trimethylsilyl)-1-naphthalenecarboxamide

Beteiligte Stoffe

Reaktionsschritte

N-Ethyl-1-naphthalenecarboxamide was reacted with 2 eq TMSCl according to General Method C. The resulting reaction mixture was worked up in the usual manner, then purified by recrystallization from cold ethyl acetate/hexanes to afford 1.6 g of desired compound as a white solid, a 58% yield. m.p. 141-143° C.

Herkunft & Nachweise