HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Chlorononane → N-phenyl-4-[N-methyl-N-(1-nonyl)amino]benzene sulfonamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Chlorononane | HCID 17185 | — |
| Edukt | N-Phenyl-4-[N-methyl-amino]benzene sulfonamide | HCID 19603974 | — |
| Lösungsmittel | Dichloromethane methanol | HCID 21226129 | — |
| Produkt | N-phenyl-4-[N-methyl-N-(1-nonyl)amino]benzene sulfonamide | HCID 19603983 | — |
Reaktionsschritte
The procedure of Example 17 was carried out using nonyl chloride and the product from Step 2 above. mp: 113-116° C.; TLC Rf =0.38 in MeOH/CH2Cl2 ; 1H NMR (CDC13, ppm) δ 7.9 (d, 2H), 7.6 (d, 5H), 7.3 (d, 2H), 7.0 (bs, 1H), 3.0 (s, 3H), 2.0 (t, 2H), 1.4 (m, 12H), 0.9 (t, 3 H)
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05994398 |
| Quelldatensatz | uspto-grants-1999_11 |
| ORD ID | ord-152ddafa642e4656805a8555514b1fdd |
| Quellennotiz | uspto-grants-1999_11 |