HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Chloroform → 2-(4-Acetylphenoxy)-2-methylpropionic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Chloroform | HCID 6212 | — |
| Edukt | 4'-Hydroxyacetophenone | HCID 7469 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Lösungsmittel | Acetone | HCID 180 | — |
| Produkt | 2-(4-Acetylphenoxy)-2-methylpropionic acid | HCID 104106 | — |
Reaktionsschritte
2-(p-Acetylphenoxy)-2-methylpropionic acid was prepared from 545 g. of p-hydroxyacetophenone, 960 g. of sodium hydroxide and 715 g. of chloroform in 11 liters of acetone according to the procedure described above in Example 1, part (d). The product was recrystallized from carbon tetrachloride and from isopropyl acetate to give 2-(p-acetylphenoxy)-2-methylpropionic acid as a pale cream solid, m.p. 108°-110°C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US03948973 |
| Quelldatensatz | uspto-grants-1976_04 |
| ORD ID | ord-43972321ca904c3ca0b13546863795ca |
| Quellennotiz | uspto-grants-1976_04 |