Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1605118Erstellt: 27. Oktober 2026

Chloroform → 2-(4-Acetylphenoxy)-2-methylpropionic acid

https://huagongshe.com/reaction/1605118

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktChloroformHCID 6212—
Edukt4'-HydroxyacetophenoneHCID 7469—
EduktSodium HydroxideHCID 14798—
LösungsmittelAcetoneHCID 180—
Produkt2-(4-Acetylphenoxy)-2-methylpropionic acidHCID 104106—

Reaktionsschritte

2-(p-Acetylphenoxy)-2-methylpropionic acid was prepared from 545 g. of p-hydroxyacetophenone, 960 g. of sodium hydroxide and 715 g. of chloroform in 11 liters of acetone according to the procedure described above in Example 1, part (d). The product was recrystallized from carbon tetrachloride and from isopropyl acetate to give 2-(p-acetylphenoxy)-2-methylpropionic acid as a pale cream solid, m.p. 108°-110°C.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS03948973
Quelldatensatzuspto-grants-1976_04
ORD IDord-43972321ca904c3ca0b13546863795ca
Quellennotizuspto-grants-1976_04