Hexadec-1-ene-1-sulfonic acid → 1-Hexadecene

HRID 1605806Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1605806
[CH:1](S(O)(=O)=O)=[CH:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]>CC(C)=O>[CH2:1]=[CH:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Komponenten

3

Edukt 1

HCID 107566Hexadec-1-ene-1-sulfonic acid

Produkt 1

HCID 123951-Hexadecene

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 180AcetoneLösungsmittel

Versuchsvorschrift

The aqueous-acetone layer which contained the sulfonic acid fraction of the product was stripped of solvents at 40°-45°C. under a vacuum to give 2.85 g. of viscous acid identified as hexadecene sulfonic acid on the basis of an IR spectrum which showed the presence of trans olefinic double bond (965 cm-1) and the absence of sultones (no 830 and 530 cm-1 bands).

Aufarbeitung

  1. customwas stripped of solvents at 40°-45°C. under a vacuum
  2. customto give 2.85 g

Quellen und Nachweise

ORD-Eintrag
ord-47b3cf032cd04a88af3fdbac6b14dce9
Quelldatensatz
uspto-grants-1976_04
Patentnummer
US03951823

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