O-ethyl N-ethyl-N-cyclohexyl-thiocarbamate → Cycloate

HRID 1606417

Reaktionsgleichung

Reaktionsgleichung von HRID 1606417
[CH2:1]([N:3]([CH:9]1[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1)[C:4](=[S:8])[O:5]CC)[CH3:2].[CH2:15](N(CCC)C(=S)OCCC)[CH2:16]C>>[CH2:1]([N:3]([CH:9]1[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14]1)[C:4](=[O:8])[S:5][CH2:15][CH3:16])[CH3:2]

Komponenten

3

Edukt 2

HCID 21542996O-ethyl N-ethyl-N-cyclohexyl-thiocarbamateHCID 22226125Propyl di-n-propylthiocarbamate

Produkt 1

HCID 14337CycloateAusbeute 80 %

Versuchsvorschrift

The procedure described in Example 4 is repeated but an equivalent amount of O-ethyl N-ethyl-N-cyclohexyl-thiocarbamate is substituted for O-propyl N,N-dipropyl-thiocarbamate. The title compound is obtaned with a yield of 80 %; b.p.: 142°-145°C/9 Hgmm., nD30 = 1.5049.

Quellen und Nachweise

ORD-Eintrag
ord-a7946ee5ba6c4aab9560df4da72b1906
Quelldatensatz
uspto-grants-1976_04
Patentnummer
US03953427

Verknüpfte Notizen

Wird geladen…