2-Methoxybenzoyl chloride → HCID 54072336, Verbindung
Reaktionsgleichung
[C:1]([O:4][C:5]1[CH:23]=[CH:22][CH:21]=[CH:20][C:6]=1[C:7]([NH:9][C:10]1[CH:18]=[C:17]([NH2:19])[CH:16]=[CH:15][C:11]=1[C:12]([OH:14])=[O:13])=[O:8])(=[O:3])[CH3:2].[CH3:24][O:25][C:26]1[CH:34]=[CH:33][CH:32]=[CH:31][C:27]=1[C:28](Cl)=[O:29]>>[C:1]([O:4][C:5]1[CH:23]=[CH:22][CH:21]=[CH:20][C:6]=1[C:7]([NH:9][C:10]1[CH:18]=[C:17]([NH:19][C:28](=[O:29])[C:27]2[CH:31]=[CH:32][CH:33]=[CH:34][C:26]=2[O:25][CH3:24])[CH:16]=[CH:15][C:11]=1[C:12]([OH:14])=[O:13])=[O:8])(=[O:3])[CH3:2]Komponenten
3
Versuchsvorschrift
By the procedure similar to that described in Example 23, 2-(2' -acetoxybenzamido)-4-aminobenzoic acid and 2-methoxybenzoylchloride were allowed to react and were treated to obtain crude crystals. Recrystallization from ethanol gave 2-(2'-acetoxybenzamido)-4-(2'-methoxybenzamido)-benzoic acid having a melting point between 197° - 198°C.
Aufarbeitung
- customto react
- additionwere treated
- customto obtain crude crystals
- customRecrystallization from ethanol