HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanol → Butyric acid (4-quinolinylmethylene)hydrazide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanol | HCID 702 | — |
| Edukt | Butyrohydrazide | HCID 77079 | — |
| Edukt | 4-Quinolinecarboxaldehyde | HCID 78072 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | Butyric acid (4-quinolinylmethylene)hydrazide | HCID 86743403 | 85,4% |
Reaktionsschritte
A mixture of 7.85 gm (0.05 mole) of 4-quinolinecarboxaldehyde, 5.11 gm (0.05 mole) of butyric acid hydrazide and 100 ml of ethanol is refluxed 4 hr. The reaction mixture is diluted with water and cooled to room temperature. The mixture is chilled. The solid that separates is collected, washed with water and dried to give 10.3 gm of the title compound, having a melting point of 130.4° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04870082 |
| Quelldatensatz | uspto-grants-1989_09 |
| ORD ID | ord-86b41a2e023d46cfa519dc8f0d867f61 |
| Quellennotiz | uspto-grants-1989_09 |