Bromomethylcyclopropane → HCID 483496, Verbindung
Reaktionsgleichung
[CH:1]([C:4]1[C:5](=[O:20])[NH:6][C:7](=[O:19])[NH:8][C:9]=1[S:10][C:11]1[CH:16]=[C:15]([CH3:17])[CH:14]=[C:13]([CH3:18])[CH:12]=1)([CH3:3])[CH3:2].Br[CH2:22][CH:23]1[CH2:25][CH2:24]1>>[CH:23]1([CH2:22][N:8]2[C:9]([S:10][C:11]3[CH:12]=[C:13]([CH3:18])[CH:14]=[C:15]([CH3:17])[CH:16]=3)=[C:4]([CH:1]([CH3:3])[CH3:2])[C:5](=[O:20])[NH:6][C:7]2=[O:19])[CH2:25][CH2:24]1Komponenten
3
Versuchsvorschrift
5-Isopropyl-6-(3,5-dimethylphenyl)thio-2,4-pyrimidinedione and bromomethyl cyclopropane were reacted by the same way with the example 1 to obtain the titled compound (170 mg, yield: 49.4%).
Quellen und Nachweise
- ORD-Eintrag
- ord-2ca16d67ddb5465d94b9b8061e966cba
- Quelldatensatz
- uspto-grants-2006_01
- Patentnummer