3,5-Dimethoxybenzyl Bromide → 1-(3,5-Dimethoxybenzyl)-5-ethyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedione

HRID 1611310

Reaktionsgleichung

Reaktionsgleichung von HRID 1611310
[CH2:1]([C:3]1[C:4](=[O:20])[NH:5][C:6](=[O:19])[NH:7][C:8]=1[C:9](=[O:18])[C:10]1[CH:15]=[C:14]([CH3:16])[CH:13]=[C:12]([CH3:17])[CH:11]=1)[CH3:2].[CH3:21][O:22][C:23]1[CH:24]=[C:25]([CH:28]=[C:29]([O:31][CH3:32])[CH:30]=1)[CH2:26]Br>>[CH3:32][O:31][C:29]1[CH:28]=[C:25]([CH:24]=[C:23]([O:22][CH3:21])[CH:30]=1)[CH2:26][N:7]1[C:8]([C:9](=[O:18])[C:10]2[CH:11]=[C:12]([CH3:17])[CH:13]=[C:14]([CH3:16])[CH:15]=2)=[C:3]([CH2:1][CH3:2])[C:4](=[O:20])[NH:5][C:6]1=[O:19]

Komponenten

3

Edukt 2

HCID 12744903,5-Dimethoxybenzyl BromideHCID 222565796-(3,5-dimethylbenzoyl)-5-ethylpyrimidine-2,4(1H,3H)-dione

Produkt 1

HCID 159577401-(3,5-Dimethoxybenzyl)-5-ethyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedioneAusbeute 50,2 %

Versuchsvorschrift

5-Ethyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedione and 3,5-dimethoxybenzyl bromide were reacted by the same way with the example 1 to obtain the titled compound (212 mg, yield: 50.2%).

Quellen und Nachweise

ORD-Eintrag
ord-3b55a3cb7e534acd9d660846565b6f3c
Quelldatensatz
uspto-grants-2006_01
Patentnummer
US06987114B1

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