9-(Chloromethyl)anthracene → 1-(9-Anthrylmethyl)-6-(3,5-dimethylphenoxy)-5-ethyl-pyrimidine-2,4-dione

HRID 1611343

Reaktionsgleichung

Reaktionsgleichung von HRID 1611343
[CH2:1]([C:3]1[C:4](=[O:19])[NH:5][C:6](=[O:18])[NH:7][C:8]=1[O:9][C:10]1[CH:15]=[C:14]([CH3:16])[CH:13]=[C:12]([CH3:17])[CH:11]=1)[CH3:2].Cl[CH2:21][C:22]1[C:23]2[C:28]([CH:29]=[C:30]3[C:35]=1[CH:34]=[CH:33][CH:32]=[CH:31]3)=[CH:27][CH:26]=[CH:25][CH:24]=2>>[CH:24]1[C:23]2[C:28](=[CH:29][C:30]3[C:35]([C:22]=2[CH2:21][N:7]2[C:8]([O:9][C:10]4[CH:11]=[C:12]([CH3:17])[CH:13]=[C:14]([CH3:16])[CH:15]=4)=[C:3]([CH2:1][CH3:2])[C:4](=[O:19])[NH:5][C:6]2=[O:18])=[CH:34][CH:33]=[CH:32][CH:31]=3)[CH:27]=[CH:26][CH:25]=1

Komponenten

3

Edukt 2

HCID 323859-(Chloromethyl)anthraceneHCID 109232665-Ethyl-6-(3,5-dimethylphenoxy)-2,4-pyrimidinedione

Produkt 1

HCID 159577751-(9-Anthrylmethyl)-6-(3,5-dimethylphenoxy)-5-ethyl-pyrimidine-2,4-dioneAusbeute 41,5 %

Versuchsvorschrift

5-Ethyl-6-(3,5-dimethylphenoxy)-2,4-pyrimidinedione and 9-chloromethyl anthracene were reacted by the same way with the example 1 to obtain the titled compound (187 mg, yield: 41.5%).

Quellen und Nachweise

ORD-Eintrag
ord-9afc833300914565a4f85ab17a5745a0
Quelldatensatz
uspto-grants-2006_01
Patentnummer
US06987114B1

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