Ammonia → HCID 10091730, Verbindung
Reaktionsgleichung
[O:1]1[C:5]([C:6]2[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=2[OH:12])=[CH:4][CH:3]=[N:2]1.[OH:13][C:14]1[CH:15]=[C:16]([CH:21]=[CH:22][CH:23]=1)[C:17](OC)=O.[NH3:24]>>[O:1]1[C:5]([C:6]2[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=2[O:12][CH2:8][CH2:7][CH2:6][CH:11]([CH3:10])[O:13][C:14]2[CH:23]=[CH:22][CH:21]=[C:16]3[C:15]=2[N:24]=[C:3]([NH2:2])[CH:4]=[CH:17]3)=[CH:4][CH:3]=[N:2]1Komponenten
4
Versuchsvorschrift
The title compound was prepared according to the procedure described in Example 92 substituting 2-isoxazol-5-ylphenol for methyl 3-hydroxybenzoate. 1H NMR (500 MHz, CDCl3) δ ppm 8.20 (d, 1H), 7.92 (d, 1H), 7.86 (dd, 1H), 7.34 (m, 1H), 7.23 (t, 1H), 7.16 (dd, 1H), 7.05 (d, 1H), 6.97 (m, 3H), 6.68 (d, 1H), 4.71 (m, 1H), 4.26 (m, 1H), 4.15 (m, 1H), 1.98–2.26 (m, 4H), 1.48 (d, 3H); MS (DCI/NH3) m/z 390 [M+H]+.
Quellen und Nachweise
- ORD-Eintrag
- ord-21e8e92c53ef4332af39bb08c7e8ccc3