Sodium Carbonate → 4-Di(3-thienyl)methoxy-1-[3-(2-nitrophenoxy)propyl]piperidine
Reaktionsgleichung
Cl.[S:2]1[CH:6]=[CH:5][C:4]([CH:7]([C:28]2[CH:32]=[CH:31][S:30][CH:29]=2)[O:8][CH:9]2[CH2:14][CH2:13][N:12]([CH2:15][CH2:16][CH2:17][O:18][C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][C:20]=3[N+:25]([O-:27])=[O:26])[CH2:11][CH2:10]2)=[CH:3]1.C(=O)([O-])[O-].[Na+].[Na+]>>[S:2]1[CH:6]=[CH:5][C:4]([CH:7]([C:28]2[CH:32]=[CH:31][S:30][CH:29]=2)[O:8][CH:9]2[CH2:10][CH2:11][N:12]([CH2:15][CH2:16][CH2:17][O:18][C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][C:20]=3[N+:25]([O-:27])=[O:26])[CH2:13][CH2:14]2)=[CH:3]1Komponenten
3
Versuchsvorschrift
The obtained hydrochloride was treated with 5% aqueous sodium carbonate to give oily 4-di(3-thienyl)methoxy-1-[3-(2-nitrophenoxy)propyl]piperidine.
Quellen und Nachweise
- ORD-Eintrag
- ord-9edd0fd0be8846d294240aabd00b8d3b
- Quelldatensatz
- uspto-grants-1993_03