1-Diphenylmethoxy-2-(4-methoxyphenethylamino)-2-methylpropane → 1-Diphenylmethoxy-2-[N-(4-methoxyphenethyl)-N-methylamino]-2-methylpropane
Reaktionsgleichung
[C:1]1([CH:7]([C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)[O:8][CH2:9][C:10]([NH:13][CH2:14][CH2:15][C:16]2[CH:21]=[CH:20][C:19]([O:22][CH3:23])=[CH:18][CH:17]=2)([CH3:12])[CH3:11])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:30]([BH3-])#N.[Na+].C=O>>[C:24]1([CH:7]([C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[O:8][CH2:9][C:10]([N:13]([CH2:14][CH2:15][C:16]2[CH:17]=[CH:18][C:19]([O:22][CH3:23])=[CH:20][CH:21]=2)[CH3:30])([CH3:11])[CH3:12])[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=1Komponenten
3
Versuchsvorschrift
The title compound was prepared as described in Example 5, Method A, using 1-diphenylmethoxy-2-(4-methoxyphenethylamino)-2-methylpropane (see Example 2) and sodium cyanoborohydride/formaldehyde. The title compound was obtained as a colourless oil (200 mg, 69%).
Aufarbeitung
- customThe title compound was prepared