2,6-Dichlorophenol → 2,6-Dichlorophenyl sulfamate

Beteiligte Stoffe

Reaktionsschritte

This compound was prepared according to the procedure of Example 84 from a mixture of 16.3 g (0.10 mole) of 2,6-dichlorophenol and 9.1 ml (0.105 mole) of chlorosulfonyl isocyanate in 75 ml of toluene to obtain 17.3 g (71%) of the title compound after recrystallization from benzene, mp 114.5°-116° C.

Herkunft & Nachweise