HCID 67496690, Verbindung → HCID 69620893, Verbindung

HRID 1628295Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1628295
[CH3:1][C:2]1[CH:7]=[C:6]([C:8]2[CH:9]=[C:10]([NH2:15])[CH:11]=[C:12]([NH2:14])[CH:13]=2)[CH:5]=[CH:4][N:3]=1.[O:16]=[C:17](NC1N=C(C2C=CN=CC=2)SC=1)[C@@H:18]([NH:26][C:27](=[O:33])[O:28][C:29]([CH3:32])([CH3:31])[CH3:30])[CH2:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1>>[NH2:14][C:12]1[CH:11]=[C:10]([NH:15][C:17](=[O:16])[C@@H:18]([NH:26][C:27](=[O:33])[O:28][C:29]([CH3:30])([CH3:31])[CH3:32])[CH2:19][C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[CH:9]=[C:8]([C:6]2[CH:5]=[CH:4][N:3]=[C:2]([CH3:1])[CH:7]=2)[CH:13]=1

Komponenten

3

Edukt 2

HCID 67496690HCID 67496690, VerbindungHCID 69620697HCID 69620697, Verbindung

Produkt 1

HCID 69620893HCID 69620893, Verbindung

Versuchsvorschrift

This title compound was prepared from 51.1C (2.10 g, 10.0 mmol) according the procedure described above for conversion of 4.A to 4.B. The product 51.1D was purified by flash chromatography on silica gel using 0-7% MeOH/CH2Cl2 for elution.

Aufarbeitung

  1. customThe product 51.1D was purified by flash chromatography on silica gel using 0-7% MeOH/CH2Cl2 for elution

Quellen und Nachweise

ORD-Eintrag
ord-8000ae479a6e40e5a413901779709bcc
Quelldatensatz
uspto-grants-2014_07
Patentnummer
US08785468B2

Notizen zur Reaktion

Wird geladen…