HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Chlorodifluoroacetic acid → 4-Nitrosotetrahydro-2H-pyran-4-yl 2-chloro-2,2-difluoroacetate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Chlorodifluoroacetic acid | HCID 66154 | — |
| Edukt | N-(oxan-4-ylidene)hydroxylamine | HCID 12298558 | — |
| Edukt | HCID 178418268 | HCID 178418268 | — |
| Produkt | 4-Nitrosotetrahydro-2H-pyran-4-yl 2-chloro-2,2-difluoroacetate | HCID 44479142 | — |
Reaktionsschritte
4-Nitrosotetrahydro-2H-pyran-4-yl 2-chloro-2,2-difluoroacetate was prepared from tetrahydro-pyran-4-one oxime, lead tetraacetate and chlorodifluoroacetic acid using conditions of General Method 3. 1H NMR (360 MHz, chloroform-d) δ 4.06-4.23 (2H, m), 3.52-3.86 (2H, m), 2.27-2.70 (2H, m), 1.72-2.07 (2H, m).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08791134B2 |
| Quelldatensatz | uspto-grants-2014_07 |
| ORD ID | ord-1c1b4ba7f0cd474687e2e64bf3ed65d6 |
| Quellennotiz | uspto-grants-2014_07 |