Carbamate → HCID 58071782, Verbindung
Reaktionsgleichung
C([O:5][C:6](=[O:25])[CH2:7][C:8]1[C:9]([CH2:23][CH3:24])=[N:10][N:11]([CH2:15][C:16]2[CH:21]=[CH:20][C:19]([NH2:22])=[CH:18][CH:17]=2)[C:12]=1[CH2:13][CH3:14])(C)(C)C.[C:26](=[O:29])([O-:28])N>>[CH2:15]([O:28][C:26]([NH:22][C:19]1[CH:18]=[CH:17][C:16]([CH2:15][N:11]2[C:12]([CH2:13][CH3:14])=[C:8]([CH2:7][C:6]([OH:5])=[O:25])[C:9]([CH2:23][CH3:24])=[N:10]2)=[CH:21][CH:20]=1)=[O:29])[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1Komponenten
3
Versuchsvorschrift
Example 3.3 was prepared according to the method described for method 3.1, employing intermediate 2.1.2 instead of intermediate 1.1.3 in the carbamate formation step. The subsequent cleavage of the tert-butyl ester was performed under acidic conditions as described for example 2.1.
Aufarbeitung
- customExample 3.3 was prepared
Quellen und Nachweise
- ORD-Eintrag
- ord-078b20d745c0412dbdc1f2fd8b104d83
- Quelldatensatz
- uspto-grants-2014_07
- DOI