Triethylamine → 1-(3,4,5-Trimethoxycinnamoyl)-4-[1-(ethylaminocarbonyl)ethyl]piperazine

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	Triethylamine	HCID 8471	—
Edukt	2-Propenoyl chloride, 3-(3,4,5-trimethoxyphenyl)-, (2E)-	HCID 112094	—
Edukt	N-Ethyl-2-(piperazin-1-yl)propanamide	HCID 13340427	—
Lösungsmittel	Chloroform	HCID 6212	—
Produkt	1-(3,4,5-Trimethoxycinnamoyl)-4-[1-(ethylaminocarbonyl)ethyl]piperazine	HCID 54340118	—

Reaktionsschritte

17.19 g of 3,4,5-trimethoxycinnamoyl chloride and 6.78 g of triethylamine are added with ice cooling to a solution of 9.54 g of 1-[1-(ethylaminocarbonyl)ethyl]piperazine in 200 ml of chloroform, and the resulting solution is kept standing at room temperature for 1 hour.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US04478838
Quelldatensatz	uspto-grants-1984_10
ORD ID	ord-97c364da0c52479d931c09a58d290af7
Quellennotiz	uspto-grants-1984_10