HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Triethylamine → 1-(3,4,5-Trimethoxycinnamoyl)-4-[1-(isopropylaminocarbonyl)ethyl]piperazin
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Triethylamine | HCID 8471 | — |
| Edukt | 2-Propenoyl chloride, 3-(3,4,5-trimethoxyphenyl)-, (2E)- | HCID 112094 | — |
| Edukt | N-isopropyl-2-(piperazin-1-yl)propanamide | HCID 13454833 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | 1-(3,4,5-Trimethoxycinnamoyl)-4-[1-(isopropylaminocarbonyl)ethyl]piperazin | HCID 54378678 | — |
Reaktionsschritte
15.15 g of 3,4,5-trimethoxycinnamoyl chloride and 8.92 ml of triethylamine are added with ice cooling and stirring to a solution of 9.80 g of 1-[1-(isopropylaminocarbonyl)ethyl]piperazine in 200 ml of chloroform, and the resulting solution is stirred at room temperature for 1 hour.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04478838 |
| Quelldatensatz | uspto-grants-1984_10 |
| ORD ID | ord-aa59b44bbc794d568f0249f8dc72d4af |
| Quellennotiz | uspto-grants-1984_10 |