3,5-Dinitrobenzoyl chloride → 3,5-Dinitrobenzohydrazide
Reaktionsgleichung
NC1C(C=[N:11][NH:12][C:13](=[O:26])[C:14]2[CH:19]=[C:18]([N+:20]([O-:22])=[O:21])[CH:17]=[C:16]([N+:23]([O-:25])=[O:24])[CH:15]=2)=NC(Cl)=C(Cl)N=1.[N+](C1C=C(C=C([N+]([O-])=O)C=1)C(Cl)=O)([O-])=O.NN>>[N+:20]([C:18]1[CH:19]=[C:14]([CH:15]=[C:16]([N+:23]([O-:25])=[O:24])[CH:17]=1)[C:13]([NH:12][NH2:11])=[O:26])([O-:22])=[O:21]Komponenten
4
Versuchsvorschrift
3,5-Dinitrobenzoic acid 2-[(3-amino-5,6-dichloropyrazinyl)methylene]hydrazide by the reaction of 3,5-dinitrobenzoyl chloride with hydrazine to form 3,5-dinitrobenzoylhydrazine, followed by the reaction of the latter with 3-amino-5,6-dichloropyrazinaldehyde.
Quellen und Nachweise
- ORD-Eintrag
- ord-08b5b59c84f04f1492d2f3fbd01512bd
- Quelldatensatz
- uspto-grants-1984_10