HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Phenylboronic Acid → N-(3-Nitro[1,1'-biphenyl]-4-yl)carbamic Acid tert-Butyl Ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Phenylboronic Acid | HCID 66827 | — |
| Edukt | Tert-butyl (4-iodo-2-nitrophenyl)carbamate | HCID 23554339 | — |
| Produkt | N-(3-Nitro[1,1'-biphenyl]-4-yl)carbamic Acid tert-Butyl Ester | HCID 57745588 | 93,2% |
Reaktionsschritte
Prepared from (4-iodo-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example A1) (994 mg, 2.73 mmol) and phenyl boronic acid (576 mg, 3.00 mmol) according to the general procedure B. Obtained as a bright yellow solid (800 mg).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06509328B1 |
| Quelldatensatz | uspto-grants-2003_01 |
| ORD ID | ord-e954a9e59f42409c97b61462711cf73f |
| Quellennotiz | uspto-grants-2003_01 |