Sodium Hydroxide → HCID 15096390, Verbindung

Reaktionsgleichung

[OH:1][CH2:2][C:3]([NH:5][CH:6]([C:12]([O:14]CC)=[O:13])[C:7]([O:9]CC)=[O:8])=[O:4].[OH-].[Na+:18]>>[OH:1][CH2:2][C:3]([NH:5][CH:6]([C:12]([O-:14])=[O:13])[C:7]([O-:9])=[O:8])=[O:4].[Na+:18].[Na+:18]

Komponenten

Edukt 2

HCID 14798Sodium Hydroxide

HCID 150963891,3-Diethyl 2-[(2-hydroxyacetyl)amino]propanedioate

Produkt 1

HCID 15096390HCID 15096390, Verbindung

Versuchsvorschrift

Diethyl 2-[(hydroxyacetyl)amino]malonate (0.56 g) is dissolved in 1N aqueous sodium hydroxide (5 ml), and the mixture is reacted at room temperature for 10 hours, and thereafter, the reaction mixture is concentrated under reduced pressure. The residue is washed with methanol to give disodium 2-[(hydroxyacetyl)amino]malonate (0.51 g).

Aufarbeitung

customthe mixture is reacted at room temperature for 10 hours
concentrationthe reaction mixture is concentrated under reduced pressure
washThe residue is washed with methanol

Quellen und Nachweise

ORD-Eintrag: ord-5ecdab6a188f4da69a6a1e8d3cec2ada
Quelldatensatz: uspto-grants-1989_11
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US04882447

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