3-Tetradecylphenol → HCID 14819672, Verbindung

HRID 1639345Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1639345
[CH2:1]([C:15]1[CH:16]=[C:17]([OH:21])[CH:18]=[CH:19][CH:20]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]>N1C=CC=CC=1.C(Cl)(Cl)Cl>[C:17]([O:21][C:17]1[CH:18]=[CH:19][CH:20]=[C:15]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14])[CH:16]=1)(=[O:21])[CH2:16][CH2:15][CH2:1][CH2:2][CH3:3]

Komponenten

4

Edukt 1

HCID 144404953-Tetradecylphenol

Produkt 1

HCID 14819672HCID 14819672, VerbindungAusbeute 195,2 %

Reagenzien, Katalysatoren, Lösungsmittel 2

HCID 1049PyridineLösungsmittelHCID 6212ChloroformLösungsmittel

Versuchsvorschrift

To a solution of 10.73 g of 3-tetradecylphenol in 30 ml of pyridine was added 8.02 g of hexanoic anyhydride. The mixture was stirred 24 hours, then diluted with chloroform, washed with water, then saturated aqueous sodium bicarbonate, dried and the solvent evaporated, giving 14.01 g of the desired compound.

Aufarbeitung

  1. washwashed with water
  2. dry with materialsaturated aqueous sodium bicarbonate, dried
  3. customthe solvent evaporated

Quellen und Nachweise

ORD-Eintrag
ord-496b323fd8c1417bb66ee540316d9556
Quelldatensatz
uspto-grants-1989_11
Patentnummer
US04883816

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