Methylamine → HCID 66737716, Verbindung
Reaktionsgleichung
[CH3:1][NH2:2].[CH3:3][O:4][C:5]1[CH:6]=[N:7][C:8]2[CH:9]=[CH:10][CH:11]=[C:12]([CH:15]=O)[C:13]=2[N:14]=1>>[CH3:3][O:4][C:5]1[CH:6]=[N:7][C:8]2[C:13]([N:14]=1)=[C:12]([CH2:15][NH:2][CH3:1])[CH:11]=[CH:10][CH:9]=2Komponenten
3
Versuchsvorschrift
Methylamine (2M in THF, 5 mL) and 3-methoxy-quinoxaline-5-carbaldehyde (0.94 g, 5 mmol, prepared according to WO 2006/021448) were coupled according to method K. The title amine was isolated as a yellowish solid (0.52 g, 51% yield).
Quellen und Nachweise
- ORD-Eintrag
- ord-9a0793d869514e77bdd00ffc73b1915e
- Quelldatensatz
- uspto-grants-2012_02
- Patentnummer
- US08114867B2
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