HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-(2,2-Dimethyl-1,3-dioxan-5-yl)ethanol → 2-(((4-(2-(2,2-Dimethyl-1,3-dioxan-5-yl)ethoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-(2,2-Dimethyl-1,3-dioxan-5-yl)ethanol | HCID 11816011 | — |
| Edukt | 2-(((4-((2-Methoxy-1,3-dioxan-5-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt | HCID 66776002 | — |
| Produkt | 2-(((4-(2-(2,2-Dimethyl-1,3-dioxan-5-yl)ethoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt | HCID 66775855 | 2% |
Reaktionsschritte
The same procedure as in the steps (6b) to (6f) of Example 6 was repeated using 2-(2,2-dimethyl-1,3-dioxan-5-yl)ethanol obtained in the step (28a) to obtain the title compound (58 mg, total yield: 2.0%) as a light yellow solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08124780B2 |
| Quelldatensatz | uspto-grants-2012_02 |
| ORD ID | ord-204a784eaa374d44828531c6683fcdf5 |
| Quellennotiz | uspto-grants-2012_02 |