Sodium Hydroxide → HCID 19802174, Verbindung

Reaktionsgleichung

[CH3:1][O:2][CH2:3][CH:4]([OH:15])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].Cl[CH2:17][C:18]([O-:20])=[O:19].[Na+].[OH-].[Na+]>>[CH3:1][O:2][CH2:3][CH:4]([O:15][CH2:17][C:18]([OH:20])=[O:19])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]

Komponenten

Edukt 3

HCID 14798Sodium Hydroxide

HCID 137094341-Methoxy-2-dodecanol

HCID 23665759Sodium chloroacetate

Produkt 1

HCID 19802174HCID 19802174, Verbindung

Versuchsvorschrift

108 g (0.5 mole) 1-methoxy-2-dodecanol are reacted with sodium chloroacetate (58.3 g; 0.5 mole) and powdered sodium hydroxide (20 g; 0.5 mole) as in Example 1 to yield 2-(1-Methoxymethylundecyloxy)acetic acid as a colourless oil, bp. 162° C./0.26 mbar, yield 59.0 g (43%).

Quellen und Nachweise

ORD-Eintrag: ord-9f4f3e6c54fe47b0a562cbe3a6427a87
Quelldatensatz: uspto-grants-1993_01
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US05176850

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