2-Chloro-1,1,1,2,3,3,3-heptafluoropropane → 1,1,1,2,3,3,3-Heptafluoropropane

HRID 1647373Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1647373
Cl[C:2]([F:11])([C:7]([F:10])([F:9])[F:8])[C:3]([F:6])([F:5])[F:4].[H][H]>[Ni]>[C:3]([CH:2]([C:7]([F:10])([F:9])[F:8])[F:11])([F:6])([F:5])[F:4]

Komponenten

4

Edukt 2

HCID 661562-Chloro-1,1,1,2,3,3,3-heptafluoropropaneHCID 178418361HCID 178418361, Verbindung

Produkt 1

HCID 679401,1,1,2,3,3,3-Heptafluoropropane

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 935NickelKatalysator2×

Versuchsvorschrift

2-Chloroheptafluoropropane (1.38 g/hr) and hydrogen (22 cc/min) were fed into the 1/4" Inconel® nickel alloy reactor filled with Inconel® nickel alloy chips (10 g). Operation at 500° C. and 250 psig for 33.3 hours gave an average of 91.3% conversion with 99.4% selectivity to CF3CHFCF3.

Quellen und Nachweise

ORD-Eintrag
ord-9d0c89fc3877409ea4126092f7fb386b
Quelldatensatz
uspto-grants-1995_07
Patentnummer
US05430204

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