Phosphorus trichloride → HCID 10520185, Verbindung
Reaktionsgleichung
[N:1]12[CH2:8][CH2:7][CH2:6][C:5]1([CH2:9][CH2:10][NH:11][C:12]1[CH:13]=[N+:14]([O-])[C:15]3[C:20]([C:21]=1[N+:22]([O-:24])=[O:23])=[CH:19][CH:18]=[CH:17][CH:16]=3)[CH2:4][CH2:3][CH2:2]2.P(Cl)(Cl)Cl>>[N:1]12[CH2:8][CH2:7][CH2:6][C:5]1([CH2:9][CH2:10][NH:11][C:12]1[CH:13]=[N:14][C:15]3[C:20]([C:21]=1[N+:22]([O-:24])=[O:23])=[CH:19][CH:18]=[CH:17][CH:16]=3)[CH2:4][CH2:3][CH2:2]2Komponenten
3
Versuchsvorschrift
3-[2-(1-Azabicyclo[3.3.0]octan-5-yl)ethyl]amino- 4-nitroquinoline 1-oxide and phosphorus trichloride were reacted in the same manner as in Example 6 to obtain the titled compound in a yield of 66.3%.
Quellen und Nachweise
- ORD-Eintrag
- ord-85d224e678a2468d9061355744f36cc1
- Quelldatensatz
- uspto-grants-1995_07
- Patentnummer
- US05434165