2,3-Dinitrotoluene → beta-Dipropylamino-2,3-dinitrostyrene

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	2,3-Dinitrotoluene	HCID 11761	—
Edukt	1-tert-Butoxy-N,N,N',N'-tetrapropylmethanediamine	HCID 13771313	—
Produkt	beta-Dipropylamino-2,3-dinitrostyrene	HCID 54130656	85,8%

Reaktionsschritte

For two hours, 5.5 g of 2,3-dinitrotoluene is heated with 13.0 g of bisdipropylamino-tert-butoxymethane to 60° C. After cooling, the reaction mixture is freed of volatile components under a high vacuum, thus obtaining 7.6 g of β-dipropylamino-2,3-dinitrostyrene as an oil.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US04925854
Quelldatensatz	uspto-grants-1990_05
ORD ID	ord-beb7c777ba3f47c29ea191bf7f02fde5
Quellennotiz	uspto-grants-1990_05