Hydrogen Bromide → Pentadecane, 7-(bromomethyl)-
Reaktionsgleichung
[CH2:1]([CH:7]([CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17])[CH2:8]O)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[BrH:18]>>[Br:18][CH2:8][CH:7]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH3:6])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17]Komponenten
3
Versuchsvorschrift
1-Bromo-2-hexyldecane was prepared by reacting 2-hexyldecanol with hydrogen bromide gas, or with 47% aqueous hydrogen bromide, according to well known procedures. The crude product was purified by distillation, b.p. 152°-154° at 18 mm of mercury.
Aufarbeitung
- distillationThe crude product was purified by distillation, b.p. 152°-154° at 18 mm of mercury
Quellen und Nachweise
- ORD-Eintrag
- ord-a40e34e60a724a1395263eb3967e5b91
- Quelldatensatz
- uspto-grants-1993_10
- Patentnummer
- US05254695
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