HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzene, 1,2,4-trichloro-3-(chloromethyl)- → 2-(2,3,6-trichlorophenylmethylthio)pyridine N-oxide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzene, 1,2,4-trichloro-3-(chloromethyl)- | HCID 74022 | — |
| Edukt | HCID 178507102 | HCID 178507102 | — |
| Produkt | 2-(2,3,6-trichlorophenylmethylthio)pyridine N-oxide | HCID 54210758 | — |
Reaktionsschritte
The intermediate 2-(2,3,6-trichlorophenylmethylthio)pyridine N-oxide is prepared from 2,3,6-trichlorobenzylchloride and 2-mercaptopyridine N-oxide sodium salt by the procedure employed in Example 3. Melting point 232° - 234°C. Yield quantitative. Structure confirmed by IR and NMR.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US03960542 |
| Quelldatensatz | uspto-grants-1976_06 |
| ORD ID | ord-14386920f37742bbbf15f8daa03ba232 |
| Quellennotiz | uspto-grants-1976_06 |