HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1659067Erstellt: 27. Oktober 2026
Thionyl Chloride → beta-(2'-Chloro-4-biphenylyl)propionyl chloride
https://huagongshe.com/reaction/1659067
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | beta-(2'-Chloro-4-biphenylyl)propionic acid | HCID 1394276 | — |
| Produkt | beta-(2'-Chloro-4-biphenylyl)propionyl chloride | HCID 21526230 | — |
Reaktionsschritte
β-(2'-chloro-4-biphenylyl)propionic acid (26 g.) is treated with thionyl chloride (18 g.) at 0°-5°C. After 10 mins the temperature is raised to 60°C for 30 mins, then the residue is distilled at 0.05 mm to give β-(2'-chloro-4-biphenylyl)propionyl chloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US03966801 |
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| Quelldatensatz | uspto-grants-1976_06 |
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| ORD ID | ord-1cf2ddcaced44d57af0b1b597587984a |
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| Quellennotiz | uspto-grants-1976_06 |
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