N-Phenylbenzimidoyl chloride → Ethyl 1,4,5,6-Tetrahydro-2-methyl-4-(2-methoxyphenyl)-5-oxo-6,7-diphenyl-1,6-naphthyridine-3-carboxylate

HRID 1659608

Reaktionsgleichung

Reaktionsgleichung von HRID 1659608
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[CH:9]1[C:14]([C:15]([O:17][CH2:18][CH3:19])=[O:16])=[C:13]([CH3:20])[NH:12][C:11]([CH3:21])=[C:10]1[C:22](OCC)=[O:23].[C:27]1([N:33]=[C:34](Cl)[C:35]2[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=2)[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1>>[CH3:20][C:13]1[NH:12][C:11]2[CH:21]=[C:34]([C:35]3[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=3)[N:33]([C:27]3[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=3)[C:22](=[O:23])[C:10]=2[CH:9]([C:4]2[CH:5]=[CH:6][CH:7]=[CH:8][C:3]=2[O:2][CH3:1])[C:14]=1[C:15]([O:17][CH2:18][CH3:19])=[O:16]

Komponenten

3

Edukt 2

HCID 264587N-Phenylbenzimidoyl chlorideHCID 9891654-(2-Meo-PH)-2,6-dimethyl-1,4-2H-pyridine-3,5-dicarboxylic acid diethyl ester

Produkt 1

HCID 20559736Ethyl 1,4,5,6-Tetrahydro-2-methyl-4-(2-methoxyphenyl)-5-oxo-6,7-diphenyl-1,6-naphthyridine-3-carboxylate

Versuchsvorschrift

This product is obtained using the procedure of Example 1 from diethyl 1,4-dihydro-4-(2-methoxyphenyl)-2,6-dimethyl-3,5-pyridine dicarboxylate and N-phenylbenzimidoyl chloride (3.1 g, 12.6%).

Aufarbeitung

  1. customThis product is obtained

Quellen und Nachweise

ORD-Eintrag
ord-f106a27dda584899a5590f14495f8f5d
Quelldatensatz
uspto-grants-1981_12
Patentnummer
US04304914

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