4-(Dimethylsulfamoyl)benzoic acid → 4-(N,N-dimethylsulfamoyl)benzoyl chloride

HRID 1663598Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1663598
[CH3:1][N:2]([CH3:15])[S:3]([C:6]1[CH:14]=[CH:13][C:9]([C:10](O)=[O:11])=[CH:8][CH:7]=1)(=[O:5])=[O:4].S(Cl)([Cl:18])=O>>[CH3:1][N:2]([CH3:15])[S:3]([C:6]1[CH:14]=[CH:13][C:9]([C:10]([Cl:18])=[O:11])=[CH:8][CH:7]=1)(=[O:5])=[O:4]

Komponenten

3

Edukt 2

HCID 145724-(Dimethylsulfamoyl)benzoic acidHCID 24386Thionyl Chloride

Produkt 1

HCID 47367944-(N,N-dimethylsulfamoyl)benzoyl chloride

Reaktionsbedingungen

Temperatur
90 °C

Versuchsvorschrift

A mixture of 4-dimethylsulfamoylbenzoic acid (688 mg) and thionyl chloride (5 mL) was stirred at 90° C. overnight. The reaction mixture was concentrated to give 4-dimethylsulfamoylbenzoyl chloride (495 mg) as a white solid.

Aufarbeitung

  1. concentrationThe reaction mixture was concentrated

Quellen und Nachweise

ORD-Eintrag
ord-1c041bcb11874842a97474a2a3d7458c
Quelldatensatz
uspto-grants-2011_10
Patentnummer
US08034949B2

Notizen zur Reaktion

Wird geladen…