HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5,8,14-Triazatetracyclo[10.3.1.02,11.04,9]hexadeca-2,4,6,8,10-pentaene → p-Toluenesulfonic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5,8,14-Triazatetracyclo[10.3.1.02,11.04,9]hexadeca-2,4,6,8,10-pentaene | HCID 170361 | — |
| Edukt | Varenicline Tosylate | HCID 86637773 | — |
| Produkt | p-Toluenesulfonic acid | HCID 6101 | — |
Reaktionsschritte
Varenicline Tosylate can be prepared by combining Varenicline base, a solvent and p-Toluene sulfonic acid (p-TSA) to obtain a reaction mixture and precipitating Varenicline Tosylate from the reaction mixture. Preferably, the obtained Varenicline Tosylate is further recovered from the reaction mixture.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08039620B2 |
| Quelldatensatz | uspto-grants-2011_10 |
| ORD ID | ord-a043c6acb8064c67afa11162b50f2adf |
| Quellennotiz | uspto-grants-2011_10 |