Trifluoroacetic acid → HCID 15175833, Verbindung
Reaktionsgleichung
C(OC([NH:8][C@H:9]([C:17]([N:19]([CH3:25])[CH2:20][C:21](OC)=[O:22])=[O:18])[CH2:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)=O)(C)(C)C.FC(F)(F)C(O)=O.C(N(CC)CC)C>CO>[CH2:10]([CH:9]1[C:17](=[O:18])[N:19]([CH3:25])[CH2:20][C:21](=[O:22])[NH:8]1)[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1Komponenten
5
Edukt 3
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
The compound obtained in Step (i) was treated with trifluoroacetic acid (30 ml), and then the resultant was heated under reflux in methanol in the presence of triethylamine to give the subtitle compound.
Aufarbeitung
- temperaturethe resultant was heated
Quellen und Nachweise
- ORD-Eintrag
- ord-9ffcc63ee46e41c8831297297d5795d1
- Quelldatensatz
- uspto-grants-2011_10
- Patentnummer
- US08044056B2
Notizen zur Reaktion
Wird geladen…