Methyl iodide → HCID 57825114, Verbindung
Reaktionsgleichung
[Br:1][C:2]1[CH:3]=[C:4]([CH2:9][CH2:10][OH:11])[CH:5]=[C:6]([Br:8])[CH:7]=1.I[CH3:13].[H-].[Na+]>>[Br:1][C:2]1[CH:3]=[C:4]([CH2:9][CH2:10][O:11][CH3:13])[CH:5]=[C:6]([Br:8])[CH:7]=1Komponenten
4
Versuchsvorschrift
In analogy to the procedure described for Building Block AW, the alkylation of 2-(3,5-dibromo-phenyl)-ethanol with iodomethane using sodium hydride as the base yielded the title compound 86% yield as a light yellow oil.
Quellen und Nachweise
- ORD-Eintrag
- ord-91eb8c64fa804e969008394faa25e362
- Quelldatensatz
- uspto-grants-2011_08
- Patentnummer
- US07989449B2
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