1-Bromo-3-methylbutane → 12-Methyltridecan-1-ol
Reaktionsgleichung
Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][OH:11].[CH3:12][CH:13]([CH3:17])[CH2:14][CH2:15]Br>>[CH3:12][CH:13]([CH3:17])[CH2:14][CH2:15][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][OH:11]Komponenten
3
Versuchsvorschrift
12-methyltridecan-1-ol was prepared from 9-bromononan-1-ol and 3-methylbutylbromide in 51% yield. The 1H NMR and MS-ESI data matched those reported by Yuasa et al. (Yuasa and Tsuruta (2004) Flavour and Fragrance Journal 19:199-204).
Quellen und Nachweise
- ORD-Eintrag
- ord-f0c13cb6cdaf40a1895ab019d1fc54a1
- Quelldatensatz
- uspto-grants-2011_08
- Patentnummer
- US07994143B2
Notizen zur Reaktion
Wird geladen…